Oxidative amidation of benzyl alcohol, benzaldhyde, benzoic acid styrene and phenyl acetylene catalyzed by HKUST-1
محل انتشار: بیست و یکمین سمینار شیمی معدنی انجمن شیمی ایران
سال انتشار: 1398
نوع سند: مقاله کنفرانسی
زبان: انگلیسی
مشاهده: 394
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شناسه ملی سند علمی:
IICC21_118
تاریخ نمایه سازی: 5 آذر 1398
چکیده مقاله:
HKUST-1-Cu synthesized in the presence and absence of P-123 through the solvothermal method (Scheme. 1). After characterization using some different microscopic and spectroscopic techniques such as XRD, FT-IR, SEM, ICP, BET and TEM its catalytic activity was investigated in the oxidative coupling of benzyl alcohol, benzaldhyde, benzoic acid, styrene and phenyl acetylene with N,N-dialkylformamides for the preparation of N,N-dimethylformamides. Different derivatives of tertiary amides were synthesized in moderate to good yields in the presence of just ~0.28 mol% of this catalytic system. Reusability of the synthesized catalysts was examined and catalysts were reusable for 8 times without a significant decrease in optimized conditions [1, 2].
نویسندگان
Haleh Moheb Ali
Chemistry Department, Tarbiat Modare University, Tehran, Iran, Tehran, Iran
Alireza Mahjoub,
Chemistry Department, Tarbiat Modare University, Tehran, Iran, Tehran, Iran
Meghdad Karimi,
Chemistry Department, Tarbiat Modare University, Tehran, Iran, Tehran, Iran
Akbar Heydari
Chemistry Department, Tarbiat Modare University, Tehran, Iran, Tehran, Iran