Novel Synthesis M-DABCO MOF by solvothermal method

The synthesis and characterization of M-DABCO serie (M = Zr) of MOF with metal salt ZrCl4 is described. Mixing of terephthalic acid (H2BDC) and 1,4-diazabicyclo [2.2.2] octane (DABCO) with metal salt ZrCl4 of mixed ligand systems to synthesize microporous MOF materials [1]. M-DABCO Synthesized were identified and characterized by fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron micrograph (SEM), Nuclear magnetic resonance (NMR) and BET.