Synthesis and Characterization of Ag2O Nanoparticles via Direct Decomposition of an Organic–inorganic Compound

An organic–inorganic compound of Ag(I) 1 containing bithiazole ligand was synthesized and characterized by spectroscopic techniques (FT-IR), 1H, 13C NMR spectroscopy and elemental analysis. Its X-ray crystallographic structure was determined. The crystal packing of this Organic–inorganic Compound was studied using geometrical analysis. The thermal stability of compound 1 has been studied by thermal gravimetric (TG) and differential thermal (DTA) analyses. The Ag2O nanoparticles has been prepared using Organic–inorganic Compound of Ag(I) 1 as precursor via thermal decomposition. As-prepared Ag2O nanoparticles were characterized by X-ray diffraction measurements (XRD), scanning electron microscopy (SEM). This study demonstrates that bithiazole complexes may be suitable precursors for preparation of nanoscale materials.

کلیدواژه ها:

Organic–inorganic ، Bithiazole ، Ag2O ، Nanoparticles ، Thermal decomposition