Hydrothermal Synthesis of Flower-Like α-Quartz Nanostructures from Iran Kaolin

سال انتشار: 1395
نوع سند: مقاله ژورنالی
زبان: انگلیسی
مشاهده: 33

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شناسه ملی سند علمی:

JR_IJCCE-35-3_004

تاریخ نمایه سازی: 17 خرداد 1404

چکیده مقاله:

Over the past many years, synthesized silica (SiO۲) has attracted wide attention because of its unique characteristics, such as low density, low thermal conductivity, high surface area, high thermal shock resistance and high specific strength. In this study, Flower-like α-quartz nano-structures have been synthesized through the hydrothermal method. The synthetic α-quartz powder was obtained using the feedstock of locally kaolin after ۱۵ h. reaction at ۱۸۰°C. The characterization of the product was investigated using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Fourier Transform InfraRed (FT-IR) spectrometer. The FT-IR spectrum of the nano-crystalline powders confirms the presence of silica. SEM studies have revealed flower-like structures consisting of nano-sheets. In the synthetic quartz, most of the population is of nano-sized and lies between ۱ µm to ۱۵ µm. This developed method has many advantages such as synthesis at low temperature and desired pH to yield superior product of desired specification.

نویسندگان

Sahar Pirkhedri

Department of Chemistry, Iran University of Science and Technology, Tehran, I.R. IRAN

Mansoor Anbia

Research Laboratory of Nanoporous Materials, Department of Chemistry, Iran University of Science and Technology, P.O. Box ۱۶۸۴۶-۱۳۱۱۴ Tehran, I.R. IRAN

Rahmatollah Rahimi

Department of Chemistry, Iran University of Science and Technology, Tehran, I.R. IRAN

Farideh Bandarchian

Department of Chemistry, Islamic Azad University, Central Tehran Branch, P.O. Box ۱۴۱۶۹ ۶۳۳۱۶ Tehran, I.R. IRAN

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