Effect of temperature and time on morphology of CuO nanoparticle during synthesis
محل انتشار: مجله بین المللی ابعاد نانو، دوره: 3، شماره: 1
سال انتشار: 1391
نوع سند: مقاله ژورنالی
زبان: انگلیسی
مشاهده: 142
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شناسه ملی سند علمی:
JR_IJND-3-1_008
تاریخ نمایه سازی: 24 تیر 1401
چکیده مقاله:
In the past decades, many methods have been developed to synthesize zero- dimensional nanoparticles, quasi–one–dimensional (۱D) CuO nanostructures, such as metal organic deposition technique, microwave irradiation, sol-gel-like dip technique, reverse micelle-assisted route, chemical method, and simple template free solution route. Among those synthesis methods, hydrothermal and chemical reaction methods are of particular interest because they are safe and environmental-friendly synthesis. By use of nonionic surfactant polyethylene glycol (PEG), the clew CuO nanostructure with the diameter of about ۴ µm was prepared at ۱۵۰˚C for ۱۱ hr. As the temperature increased to ۱۶۰C for ۱۱ hr, the gear wheel CuO nanostructure with the diameter of about ۷۰ nm was made. Furthermore, two other temperatures (۱۸۰ and ۲۰۰) are utilized for ۲۰ hr to produce nanowire. The product was characterized by powder X-Ray diffraction, and scanning electron microscopy SEM showed the various shapes of CuO nanostructures, including clew, gearwheel, and nanowire bundles.
کلیدواژه ها:
نویسندگان
S. Sabbaghi
Nano Chemical Engineering Dep. of Shiraz University, shiraz, Iran.
H. Orojlou
Nano Technology Research Institute, Shiraz University, Shiraz, Iran.
M. R. Parvizi
Research and Development of Boualisina petrochemical company,Mahshahr, Iran.
R. Saboori
Nano Technology Research Institute, Shiraz University, Shiraz, Iran.
M. Sahooli
Nano Chemical Engineering Dep. of Shiraz University, shiraz, Iran.