A magnetic graphitic carbon nitride as a new adsorbent for simple separation of Ni (II) ion from foodstuff by ultrasound-assisted magnetic dispersive-micro solid phase extraction method

سال انتشار: 1398
نوع سند: مقاله ژورنالی
زبان: انگلیسی
مشاهده: 407

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شناسه ملی سند علمی:

JR_AMECJ-1-1_006

تاریخ نمایه سازی: 3 اسفند 1398

چکیده مقاله:

In this research, a magnetic graphitic carbon nitride (g-C3N4-SnFe2O4) was successfully synthesized and utilized as an efficient adsorbent for nickel (Ni2+) separation/extraction from vegetable samples by ultrasound-assisted magnetic dispersive micro solid-phase extraction (UA-M-D-μSPE). After separation and preconcentration step, Ni ions were determined via micro-sampling flame atomic absorption spectrometry (MS-FAAS). A successful synthesis of g-C3N4- SnFe2O4 was investigated by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and vibrating sample magnetometer (VSM). The optimization of adsorption and desorption steps was effectively studied by the on-at-a time method. In addition, under the optimum experimental conditions, the limits of detection (LODs), the linear ranges (LR) and relative standard deviations (RSDs%, for n = 5) were obtained 1.0 μgL−1, 4.0 ─ 500.0 μgL−1, and 1.4respectively.

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نویسندگان

Bahareh Fahimirad

Department of Chemistry, Semnan University, Semnan, Iran

Alireza Asghari

Department of Chemistry, Semnan University, Semnan, Iran