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Synthesis of Mesoporous MgAl2O4 Spinel Nanopowder with High Surface Area

عنوان مقاله: Synthesis of Mesoporous MgAl2O4 Spinel Nanopowder with High Surface Area
شناسه ملی مقاله: ICHEC07_468
منتشر شده در هفتمین کنگره ملی مهندسی شیمی در سال 1390
مشخصات نویسندگان مقاله:

z Mosayebi - Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan, Iran
m Rezaei - Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan, Iran Catalyst and Advanced Materials Research Laboratory, Chemical Engineering Department, Faculty of Engineering, University of Kashan, Kashan, Iran
n hadian - Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan, Iran
f meshkani - Catalyst and Advanced Materials Research Laboratory, Chemical Engineering Department, Faculty of Engineering, University of Kashan, Kashan, Iran

خلاصه مقاله:
In this research, mesoporous nanocrystallite magnesium aluminate powder with high specific surface area was synthesized by a simple co-precipitation method with the addition of pluronic P123 triblock copolymer as surfactant. The prepared samples were characterized by X-ray Diffraction (XRD), N2 adsorption (BET) and Scanning electron microscopy (SEM). The effects of calcination temperature on the structural properties of the samples were investigated. The results showed that with increasing in calcination temperature from 600 to 800 ˚C increased the crystallite sizes and decreased the specific surface area in the range of 183-124 m2g-1.

کلمات کلیدی:
Magnesium aluminate, Nanopowder, Precipitation, Surfactant

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/341219/