M. Palizdar - R;D and Training Department, CPG Industrial, Mining and Technical Services, Germany
Z. Aslam - Institute for Materials Research, Leeds University, U.K.
R. Aghababazadeh - dvanced Materials and Nanotechnology Department, Materials and Energy Research Center, Iran
A. Mirhabibi - ۴Centre of Excellence for Advanced Materials and Processing (CEAMP), Iran University of Science and Technology, Iran/۲Institute for Materials Research, Leeds University, U.K
P. Sangpour - Advanced Materials and Nanotechnology Department, Materials and Energy Research Center, Iran
Z. Abadi - dvanced Materials and Nanotechnology Department, Materials and Energy Research Center, Iran
Y. Palizdar - Advanced Materials and Nanotechnology Department, Materials and Energy Research Center, Iran
R. Brydson - ۲Institute for Materials Research, Leeds University, U.K

In this paper the chemical interaction between catalyst and support has been studied to understand the observed different growth rate of CNTs in our previous paper. Both pure MgO and Mg(NO۳)۲ . ۶H۲O as sources of the MgO catalyst support and Fe۲(SO۴)۳ · xH۲O as the source of the Fe catalyst, were employed. A Fe catalyst supported on MgO has been synthesized using the wet impregnation method followed by calcination. To compare the catalyst grain size and its distribution, the sample were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray powder diffraction (XRD) and BET specific surface area (SSA) measurement and X-ray photoelectron spectroscopy (XPS). XPS technique have utilized complementary to demonstrate the existence of chemical interaction between MgO support and Fe catalyst. Results revealed that the type of precursor used to prepare the support has a significant influence on the morphology of the support and the associated distribution of the Fe catalysts. The highest yield of MgFe۲O۴ phase was obtained using a pure MgO precursor which after calcination results in a homogenous distribution of nano-sized Fe particles over the support surface

Catalyst, Support, Magnesium ferrite