Organo-Clay Composites of Intercalated ۴-Methylaniline and Its Schiff Base Derivative: Preparation and Characterization
- سال انتشار: 1401
- محل انتشار: مجله علوم دارویی و شیمی، دوره: 5، شماره: 6
- کد COI اختصاصی: JR_JMCH-5-6_022
- زبان مقاله: انگلیسی
- تعداد مشاهده: 188
نویسندگان
Department of Chemistry, College of Science, University of Baghdad, Baghdad, Iraq
Department of Chemistry, College of Science, University of Baghdad, Baghdad, Iraq
Department of Chemistry, College of Education for Pure Sciences Ibn-Alhaitham, University of Baghdad, Baghdad, Iraq
Department of Chemistry, College of Education for Pure Sciences Ibn-Alhaitham, University of Baghdad, Baghdad, Iraq
چکیده
۴-methylaniline and its Schiff base derivative were intercalated into the Bentonite clay interlayers in a solid state reaction followed by a condensation reaction to produce two organo-clay composites. X-ray diffraction was used to identify the changes in basal spacing of montmorillonite layers which exhibited noticeable alteration before and after the formation of the composites. FT-IR spectra, on the other hand, were utilized for identifying the structural compositions of the prepared materials as well as the formation of the intercalated Schiff base derivative. The surface morphology of the composites was examined by Scanning Electron Microscopy SEM and Atomic Force Microscope AFM, which reflected some differences in the surface of prepared composites as the particle size decreased with the Schiff base formation.کلیدواژه ها
Schiff base, p-toluidine, Bentonite, Intercalation, organo-clay compositeاطلاعات بیشتر در مورد COI
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